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Water-Washable and Post-Emulsified Penetrants

February 8, 2012
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Although Liquid Penetrant Inspection is recommended for the detection of all types of surface fl aws, the selection and use of the penetrant is going to depend on a number of factors.

A liquid penetrant inspection under black light shows the detection of surface flaws. Source: Magnaflux


If working to any specification, whether military or private, the penetrant selection for a process will be spelled out. Other selection criteria include the surface and configuration of the part to be tested. Also, the size and location of the defect determines the sensitivity level required. Also, how critical is the function of the part to be inspected, such as used in rotating or moving components, and is it subject to excessive heat.

All penetrant materials do not perform the same and are not designed to do so. Different formula-tions have been developed to address a variety of inspection applications. For the purpose of this dis-cussion, we will look at both water-washable and post-emulsified penetrants.



As pictured, the liquid penetrant will fluoresce under black light. Source: Magnaflux

Water-Washable Penetrants

Water-washable penetrants (Method A) are available as Fluorescent (Type 1) or Visible (Type 2) pene-trants and in all sensitivity levels. The water-wash method is popular for several reasons. It is less ex-pensive, the process time is quicker, there are fewer processing steps and timing variables are reduced.

Water-washable penetrants work best on rough surface parts, threaded or grooved parts and those with holes and orifices, which may be difficult to remove with the post emulsification method. It is es-pecially suitable for automation, larger parts, leak testing and use on parts that are incompatible with oil-based systems.

Water-washable penetrants are removed by manual or automated water spray, manual wipe or air agitated immersion wash. If a manual spray is used, the water pressure should not exceed 40 psi; the temperature should be between 50 –100 F using a coarse spray at a minimum distance of 12 inches. Al-though water washable processing has its advantages, certain specifications will restrict its use because over-washing can occur in shallow discontinuities, which makes rinsing time critical to the process.



Recommended Developers for Water-Washable Penetrants

Developers increase the visibility of both the visible and fluorescent penetrants. They draw the pene-trant out of the flaws and spread the indication for brighter results. The developer you choose should be able to provide a good, uniform contrast; be easy to apply and remove; and work well with the penetrant chosen.

Dry developers are the most effective for fluorescent water-washable penetrants. It is the easiest developer to apply. However, before using a dry developer, it is important that the part be completely dried after the rinse before applying the dry powder. It can be applied by immersion or by dusting with hand-held powder bulbs. In automated systems, developers are applied in a swirl cloud developer sta-tion. The use of a dust collector to evacuate the powder from the chamber is also recommended. A non-aqueous developer is a convenient solvent developer for portable fluorescent aerosol penetrant inspec-tions.

Water-soluble developers are not recommended for use with water-washable penetrants because it is possible that when used with these penetrants, it will act as an additional emulsifier and wash the penetrant away. Many specs will prohibit the use of these developers with water washable penetrants.

With visible water-washable penetrants, a non-aqueous or solvent developer is recommended be-cause it gives the best contrast to the penetrant.





Advantages to Water-Washable Penetrant

  • Lower cost (no emulsifier needed)

  • Fewer processing steps

  • Process time reduced

  • Variables associated with PE dwell time eliminated





  • Disadvantages to Water-Washable Penetrant

  • Over washing can occur in shallow defects

  • Water rinsing time is critical

  • Water contamination is susceptible



  • Post-Emulsifiable Penetrants

    When removal of the penetrant from the defect due to over-washing of the part is a concern, a post-emulsifiable penetrant system can be used. These parts are usually smoothed surfaced and perform critical functions that require higher sensitivity to smaller defects. Post-emulsifiable penetrants require a separate emulsifier to break the penetrant down and make it water washable. Method C relies on a sol-vent cleaner to remove the penetrant from the part being inspected. Method B and D penetrants require an additional processing step where a separate emulsification agent is applied to make the excess penetrant more removable with a water wash. Lipophilic emulsification systems are oil-based materials that are supplied in ready-to-use form. Hydrophilic systems are water-based and supplied as a concentrate that must be diluted with water prior to use.



    Emulsifiers

    Lipophilic emulsifiers (Method B) were introduced in the late 1950s and work with both a chemical and mechanical action. After the emulsifier has coated the surface of the object, mechanical action starts to remove some of the excess penetrant as the mixture drains from the part. During the emulsification time, the emulsifier diffuses into the remaining penetrant and the resulting mixture is easily removed with a water spray.

    Hydrophilic emulsifiers (Method D) also remove the excess penetrant with mechanical and chemi-cal action but the action is different because no diffusion takes place. Hydrophilic emulsifiers are basi-cally detergents that contain solvents and surfactants. The hydrophilic emulsifier breaks-up the pene-trant into small quantities and prevents these pieces from recombining or reattaching to the surface of the part. The mechanical action of the rinse water removes the displaced penetrant from the part and causes fresh remover to contact and lift newly exposed penetrant from the surface.

    The hydrophilic post-emulsifiable method is more sensitive than the lipophilic post emulsifi-able method and has made the latter method virtually obsolete. The major advantage of hydrophilic emulsifiers is that they are less sensitive to variation in the contact and removal time. While emulsifica-tion time should be controlled as closely as possible, a variation of one minute or more in the contact time will have little effect on flaw detectability when a hydrophilic emulsifier is used. However, a variation of as little as 15 to 30 seconds can have a significant effect when a lipophilic system is used.





    Advantages of the Post-Emulsifiable Penetrant Process

  • Higher sensitivity to smaller defects

  • Shows wide, shallow defects

  • More controlled removal of surface penetrants





  • Disadvantages of the Post-Emulsifiable Penetrant Process

  • Extra processing step

  • Emulsification time control is critical

  • Penetrant removal is difficult in threaded parts, holes and slots

  • Not good on rough surfaces NDT



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